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#111 Laboratory for Organothiophosphorus Compounds (LOTPC)

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Head of the Laboratory, Doctor of Sciences Odinets Irina Leonovna

(phone +7-499-135-9356, +7-499-135-6373; e-mail: )

 

Staff:

Aladzieva I.M., Aleksanyan D.V., Alexenko V.Yu., Artyushin O.I., Bykhovskaya O.V., Vinogradova N.M., Genkina G.K., Kalyanova R.M., Kozlov V.A., Makarov M.V., Matveeva E.V., Sharova E.V.

 

Subjects of investigations:

Development of the organophosphorus synthesis methodology including “green chemistry” procedures (synthesis in ionic liquids, water and/or under phase catalysis conditions) resulting in organophosphorus compounds of practical importance having bioactivity or complexing properties; investigations of reaction peculiarities, stereochemistry and mechanisms of new type rearrangements, polymerizations, intra- and intermolecular cyclizations in the series of functionalized organophosphorus compounds; coordination chemistry of oligodentate ligands and investigation of catalytic, luminescent and magnetochemical properties of metal complexes.

 

Main publications 2009-2011 :

1. M. I. Kabachnik. Chemistry of the Organophosphorus compounds. Selected Proceedings, in 3 volumes (publishers М.: NAUKA, 2008-2009).

2. Irina L. Odinets, Oleg. I. Artyushin, Nikolay Shevchenko, Pavel V. Petrovskii, Valentin G. Nenaidenko, Gerd-Volker Röschenthaler. Efficient synthesis of substituted cyclic a-aminophosphonates. Synthesis, 2009, 4, 577-582.

3. Michael V.Makarov, Ekaterina Yu. Rybalkina, Gerd-Volker Röschenthaler, Kurt W. Short, Tatiana V. Timofeeva, Irina L.Odinets. Design, cytotoxic and fluorescent properties of novel N-phosphorylalkyl substituted E,E-3,5-bis(arylidene)piperid-4-ones. Eur.J.Med.Chem., 2009, 44(5), 2135-2144.

4. I.L. Odinets, O.I. Artyushin, S.N.Osipov, G.-V. Röschenthaler, “Propargyl Substituted Phosphonocarboxylates. Efficient Synthesis and Application for Click Chemistry”. Synthesis, 2009, 21, 3579-3588.

5. I.M. Aladzheva, O.V. Bykhovskaya, Y.V.Nelyubina, A.A. Korlyukov, P.V. Petrovskii, I.L. Odinets. Facile one-pot synthesis and X-ray characterization of N-(thio)phosphoryl-2-oxo-1,2-azaphospholanes: first example of cyclic O,O- and O,S-bidentate ligands with the P-N-P backbone, Synthesis, 2010, 613-618.

6. I.L. Odinets, E.V. Sharova, O.I.Artyshin, K.A. Lyssenko, Yu.V. Nelyubina, G.V.Мyasoedova, N.P.Molochnikova, E.A.Zakharchenro. Novel class of functionalized ionic liquids with grafted CMPO-moieties for actinides and rare-earth elements recovery. Dalton Trans., 2010, 39, 4170 — 4178.

7. V.A. Kozlov, D.V. Aleksanyan, Yu.V. Nelyubina, K.A. Lyssenko, P.V. Petrovskii, I.L. Odinets. Cyclopalladation of meta-Diphenylthiophosphoryloxybenzaldimines: NCS and unexpected NCO 5,6-Membered Pincer Palladium Complexes. Organometallics, 2010, 29(9), 2054-2062.

8. I. L. Odinets, E.V. Matveeva. “Green” solvents in organophosphorus synthesis (review). Current Organic Chem., 2010, 14(12), 1171-1184.

9. V. A. Kozlov, D.V. Aleksanyan, Yu.V. Nelyubina, K.A. Lyssenko, P.V. Petrovskii, A.A. Vasil’ev, I.L. Odinets. Hybrid Thiophosphoryl-Benzothiazole Palladium SCN-Pincer Complexes: Synthesis and Effect of Structure Modifications on Catalytic Performance in the Suzuki cross-coupling. Organometallics, 2011; 30(11), 2920-2932

10. I. M. Aladzheva, O.V. Bykhovskaya, Y.V. Nelyubina, P.V. Petrovskii, Z.S. Klemenkova, I.L. Odinets Uranium Complexes of cyclic O,O-bidentate ligands with the P-N-P backbone. Inorg.Chim.Acta, 2011, 373, 130-136

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